The steps were as follows: trimethyl borate-10 was synthesized from boron-10 trifluoride-ether complex and sodium methylate, which was hydrolyzed to synthetize boric-10 acid. 首先采用***-10-乙醚络合物与甲醇钠反应生成硼-10酸三甲酯,之后水解合成硼-10酸。
Preparation of Sodium Methylate with Sodium 利用金属钠制备甲醇钠的生产工艺
Solid sodium methylate ( 98%) was manufactured from methanol solution of sodium methylate ( 27%~ 31%). Some influential factors impacting on product qualities, such as the kinds of the medias of solution, proportion, vaccum and temperature, were studied. 以甲醇钠甲醇溶液(27%~31%)为原料制备固体甲醇钠(98%),研究了溶媒种类、配比、真空度、温度控制对产品质量的影响。
The glucosamine hydrochloride reacted with sodium methylate to produce glucosamine base. 氨基葡萄糖盐酸盐先与甲醇钠反应生成氨基葡萄糖碱,再与三氧化硫反应,得白色粉末状产品。